Determination of Zirconium in Plutonium by Ion Exchange and Spectrography
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چکیده
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determination of olanzapine and thiourea using electrodes modified by dna and film of copper-cobalt hexacyanoferrate & investigation of electro-oxidation of some catechol derivatives in the presence of 4-phenylsemicarbazid
چکیده هدف از این کار بررسی الکترواکسیداسیون کتکول و مشتقات آن در حضور 4-فنیل سمی کاربامازید بوده است اکسیداسیون کتکولها ترکیبات نا پایدار کینونها را تولید می کنند که این ترکیبات می تواند در واکنش مایکل بعنوان پذیرنده نوکلئوفیل عمل نمایند. در ادامه اکسایش کتکولهای (a-c1) را درحضور 4-فنیل سمی کاربامازید در محلول آب/استونیتریل (90/10)بوسیله ولتامتری چرخه ای و کولن متری در پتانسیل ثابت مورد بررسی ...
15 صفحه اولRapid Determination of Lead in Urine by Ion Exchange.
For routine screening of employees in the lead industry, a method for determination of urinary lead was developed in which this element is removed from urine by means of a chelating agent, eluted, and determined by a modified dithizone method. The method gives values which are about 5% below those obtained by the wet ashing technic, with a precision of ± 2.1% in the range of 2-15 jig. of lead p...
متن کاملDetermination of D - and ~ Amino Acids by Ion Exchange
A procedure for the precise determination of the D and L isomers in a given sample of an amino acid has been based upon chromatographic separation of the diastereoisomeric dipeptides obtained by derivatization with an L-amino acid N-carboxyanhydride. The conditions for the preparation of dipeptides developed by Hirschmann and associates make the derivatization step simple and rapid; the couplin...
متن کاملRapid Determination of Plasma Ammonia by an Ion-exchange Technic.
A method is described for the colorimetric determination of ammonia in plasma by a batch ion-exchange procedure. The method combines separation of ammonium ion, using a strongly acidic cation-exchange resin, with a sensitive colorimetric procedure which simultaneously elutes and colorimetrically reacts with the ammonium ion to produce a stable color. Interference by basic amino acids is negligi...
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ژورنال
عنوان ژورنال: Applied Spectroscopy
سال: 1959
ISSN: 0003-7028,1943-3530
DOI: 10.1366/000370259774615167